Tetracarbonylbis[(pentafluoroethyl)diphenylphosphine]chromium(0)
✍ Scribed by Peters, R. Gregory ;Golynskiy, Misha V. ;Baughman, Russell G.
- Publisher
- International Union of Crystallography
- Year
- 2002
- Tongue
- English
- Weight
- 257 KB
- Volume
- 58
- Category
- Article
- ISSN
- 1600-5368
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📜 SIMILAR VOLUMES
Single-crystal X-ray study T = 178 K Mean '(C±C) = 0.005 A Ê R factor = 0.040 wR factor = 0.108 Data-to-parameter ratio = 13.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
The title compound, trans-[RhCl(C 18 F 15 P) 2 (CO)], crystallizes with one independent molecule in the asymmetric unit. Important geometric parameters are Rh-P = 2.2797 ( 14) and 2.2993 (14) A ˚, Rh-Cl = 2.3642 (12) A ˚, Rh-C = 1.824 (4) A ˚, C-Rh-Cl = 174.12 (13) , P-Rh-C = 91.73 (13) and 93.71 (1
Single-crystal X-ray study T = 296 K Mean '(C±C) = 0.015 A Ê R factor = 0.047 wR factor = 0.111 Data-to-parameter ratio = 12.6 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Single-crystal X-ray study T = 294 K Mean '(C±C) = 0.007 A Ê R factor = 0.049 wR factor = 0.069 Data-to-parameter ratio = 20.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.