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Systematics in simulation of the cross-peak fine structure in 2D and 3D NMR spectroscopy

✍ Scribed by Imke Bock-Möbius

Publisher
Elsevier Science
Year
1989
Weight
385 KB
Volume
84
Category
Article
ISSN
0022-2364

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Fine Structure of the P–H5′ Cross-Peak i
Fine Structure of the P–H5′ Cross-Peak in 31P–1H Correlated 2D NMR Spectroscopy. An Efficient Probe for the Backbone Torsion Angles β and γ in Nucleic Acids
✍ Jeroen A. Pikkemaat; Cornelis Altona 📂 Article 📅 1996 🏛 John Wiley and Sons 🌐 English ⚖ 701 KB

The splitting pattern of the P-H5" (and P-H5') cross-peak in a 2D 31P-1H correlated NMR spectrum is analysed. Since this cross-peak pattern is strongly dependent on two coupling constants, 'J(PH5") and 3J(H4H5"), it is an efficient probe for the backbone torsion angles fl and y in nucleic acids. A m