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Synthetic Studies Toward Pectenotoxin 2. Part II. Synthesis of the CDE and CDEF Ring Systems

✍ Scribed by Helmboldt, Hannes; Aho, Jatta E.; Pihko, Petri M.

Book ID
126909557
Publisher
American Chemical Society
Year
2008
Tongue
English
Weight
475 KB
Volume
10
Category
Article
ISSN
1523-7060

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The EFGH ring segment of gambierol was synthesized from 2-deoxy-D-ribose in 40 steps. The present synthesis includes a SmI 2 -mediated reductive cyclization and a Pd-catalyzed coupling of enol triflate with a zinc bis-homoenolate as key steps.

ChemInform Abstract: Synthetic Studies T
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