✦ LIBER ✦

Synthesis of Vitamin B 6

✍ Scribed by Harris, Stanton A.; Folkers, Karl.

Book ID: 118229633
Publisher: American Chemical Society
Year: 1939
Tongue: English
Weight: 332 KB
Volume: 61
Category: Article
ISSN: 0002-7863
DOI: 10.1021/ja01874a069

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## Abstract 3‐Hydroxy‐4‐(hydroxymethyl)‐5‐(hydroxymethyl‐d~2~)‐2‐methylpyridine(pyridoxine‐d~2~) was prepared by reduction of α^4^‐3‐0‐isopropylidene‐5‐pyridoxic acid with lithium aluminum deuteride. Deuterium was inserted in the 2‐methyl group using base catalyzed exchange between deuterium oxide