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Synthesis of Vitamin B 6 . III. 3-Deoxypyridoxine

✍ Scribed by Harris, Stanton A.; Harris, Elbert E.; Peterson, Elwood R.; Rogers, Edward F.


Book ID
118743645
Publisher
American Chemical Society
Year
1967
Tongue
English
Weight
243 KB
Volume
10
Category
Article
ISSN
0022-2623

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## Abstract Attempts are described to simplify the synthesis of vitamin B~6~ by a simultaneous reduction of the ester groups and reductive elimination of the chlorine atom in dimethyl 3‐amino‐6‐chloro‐2‐methylpyridine‐4,5‐dicarboxylate (III) with lithium aluminium hydride. After prolonged refluxing