Synthesis of Thiophosphoryl Difluoride Isothiocyanate and Thiophosphoryl Fluoride Diisothiocyanate
β Scribed by Dr. H. W. Roesky
- Publisher
- John Wiley and Sons
- Year
- 1967
- Tongue
- English
- Weight
- 118 KB
- Volume
- 6
- Category
- Article
- ISSN
- 0044-8249
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## Abstract A series of phosphorylated and thiophosphorylated compounds of 2βsubstituted benzimidazoles have been synthesized by the reaction of POCl~3~ and PSCl~3~ with 2βsubstituted benzimidazoles in different molar ratios. The compounds have been characterized by elemental analyses, infrared, an
## Abstract A convenient and practical method for the preparation of __N__βthiophosphoryl imines was developed through the thermal condensation of acetals with different thiophosphoramides at 120β160Β°C. Β© 2008 Wiley Periodicals, Inc. Heteroatom Chem 19:238β244, 2008; Published online in Wiley Inter