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Preparation of Phosphoryl Difluoride Isothiocyanate and Phosphoryl Fluoride Diisothiocyanate

✍ Scribed by Dr. H. W. Roesky

Publisher
John Wiley and Sons
Year
1967
Tongue
English
Weight
118 KB
Volume
6
Category
Article
ISSN
0044-8249

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A Practical Preparation of Diisopropyl Phosphoryl Protected Amino Acids. -Slow addition of hypochlorite to an alkaline solution of an amino acid (I) and (IV) and diisopropylphosphite (I) allows the preparation of N-diisopropyl phosphoryl protected amino acids (III) and (V) without racemization. -(B