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Synthesis of the β-D-glucosyl ester of [carbonyl-13C]-indole-3-acetic acid

✍ Scribed by Andreja Jakas; Volker Magnus; Stefica Horvat; Göran Sandberg

Publisher
John Wiley and Sons
Year
1993
Tongue
French
Weight
339 KB
Volume
33
Category
Article
ISSN
0022-2135

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✦ Synopsis

Abstract

An efficient, operationally simple synthetic approach to 1‐O‐([carbonyl‐^13^C]‐indole‐3′‐ylacetyl)‐β‐D‐glucopyranose is described. The synthesis was carried out by fusing a fully benzylated 1‐O‐glucosylpseudourea intermediate with [carbonyl‐^13^C]‐indole‐3‐acetic acid, followed by hydrogenolytic removal of the protective groups.

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