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Synthesis of the Key Precursor of Hirsutellide A

โœ Scribed by Xu, Yanjie; Duan, Xuemin; Li, Meiling; Jiang, Liqin; Zhao, Guangle; Meng, Yi; Chen, Ligong

Book ID
121293577
Publisher
Molecular Diversity Preservation International
Year
2005
Tongue
English
Weight
183 KB
Volume
10
Category
Article
ISSN
1420-3049

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## Abstract For Abstract see ChemInform Abstract in Full Text.

An asymmetric synthesis of the key precu
An asymmetric synthesis of the key precursor to (โˆ’)-indolizomycin
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Using chiral bicyclic lactams, containing an oc,fi-unsaturation, the key precursor of (-)-indolizomycin was obtained in optically pure form. The sequence involved a >20:1 diastereoselective cyclopropanation of the unsaturated lactam 5 employing sulfoxonium methylide. Tic14 mediated addition of allyl