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Synthesis of the C(1)–C(16) fragment of bryostatins using an ‘ene’ reaction between an allylsilane and an alkynone

✍ Scribed by Matthew O’Brien; Eric J. Thomas

Book ID
113928958
Publisher
Elsevier Science
Year
2011
Tongue
French
Weight
732 KB
Volume
67
Category
Article
ISSN
0040-4020

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An approach towards the C1–C16 fragment
An approach towards the C1–C16 fragment of antineoplastic macrolide bryostatins by kinetic resolution of a racemic terminal epoxide using Jacobsen's catalyst
✍ J.S Yadav; A Bandyopadhyay; A.C Kunwar 📂 Article 📅 2001 🏛 Elsevier Science 🌐 French ⚖ 134 KB

A stereo-and enantioselective approach towards the C 1 -C 16 fragment of bryostatins is reported using Jacobsen's catalyst for kinetic resolution of a terminal epoxide, a Horner-Wadsworth-Emmons coupling reaction and a 1,4-Michael type cyclization as key steps.