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Synthesis of the C17C27 fragment of bryostatin 3

✍ Scribed by Tetsuo Obitsu; Ken Ohmori; Yasuyuki Ogawa; Hiroyuki Hosomi; Shigeru Ohba; Shigeru Nishiyama; Shosuke Yamamura

Book ID
108387028
Publisher
Elsevier Science
Year
1998
Tongue
French
Weight
230 KB
Volume
39
Category
Article
ISSN
0040-4039

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Synthesis of the C(1)C(16) fragment of
Synthesis of the C(1)C(16) fragment of bryostatins
✍ Matthew O'Brien; Nicholas H Taylor; Eric J Thomas 📂 Article 📅 2002 🏛 Elsevier Science 🌐 French ⚖ 87 KB

A synthesis of the C(1) C( 16) fragment 43 of the bryostatins is reported which features a stereoselective equivalent of an 'ene' reaction between the allylsilane 35 and the alkynone 33 and the stereoselective conjugate addition-cyclisation of the dienyl ketone 36 to give the acetal 39 after acetali