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Synthesis of retinals labelled at positions 14 and 15 (with 13C and/or 2H)

✍ Scribed by J. A. Pardoen; C. Winkel; P. P. J. Mulder; J. Lugtenburg


Publisher
Elsevier Science
Year
2010
Tongue
English
Weight
689 KB
Volume
103
Category
Article
ISSN
0165-0513

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## Abstract Efficient methods for synthesising L‐[methy‐ ^13^C]methionine from [^13^C]iodomethane and L‐methionine, and L‐[3,4‐^13^C~2~] methionine from [^13^C~2~]ethene, are described; the preparation of [3,3‐^2^H~2~]methionine and [2,3,3‐^2^H~3~]methionine from methionine by an exchange method is