𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Synthesis of Phenyl-13C6-ethene

✍ Scribed by Elizabeth M. Zippi

Publisher
John Wiley and Sons
Year
2001
Tongue
French
Weight
72 KB
Volume
44
Category
Article
ISSN
0022-2135

No coin nor oath required. For personal study only.

✦ Synopsis

Abstract

In an effort to prepare an improved carbon‐rich target material for the accelerator production of ^13^N labelled ammonia for use in positron emission tomography (PET), sulfonated poly(styrene/divinylbenzene) has been evaluated. The preparation of this target material using naturally abundant carbon‐12 compounds was investigated in an effort to optimize conditions for the preparation of the analogous carbon‐13 target material which may provide a cost‐effective method for producing nitrogen‐13 labelled ammonia via proton irradiation. As part of this study, phenyl‐13C6‐ethene was synthesized in three steps starting from benzene‐13C6. Copyright © 2001 John Wiley & Sons, Ltd.

📜 SIMILAR VOLUMES

Synthesis of 1-phenyl-2-phenyl-1-13C-eth
Synthesis of 1-phenyl-2-phenyl-1-13C-ethene-1-13C (trans-stilbene) and derivatives
✍ Gary A. Braden; Ulrich Hollstein 📂 Article 📅 1976 🏛 John Wiley and Sons 🌐 French ⚖ 431 KB

## Abstract For mass spectrometric studies 1‐phenyl‐2‐phenyl‐1‐^13^C‐ethene‐1‐^13^C (trans‐stilbene) was synthesized from acetic‐1‐^13^C acid and acetic‐2‐^13^C acid via methylcyclohexene‐1‐^13^C and ‐α‐^13^C and toluene‐1‐^13^C and ‐α‐^13^C. No scrambling of the label was observed during the aroma

Synthesis of [phenyl-13C6]lachnanthocarp
Synthesis of [phenyl-13C6]lachnanthocarpone and other 13C-labelled phenylphenalenones
✍ Felipe Otálvaro; Winston Quiñones; Fernando Echeverri; Bernd Schneider 📂 Article 📅 2004 🏛 John Wiley and Sons 🌐 French ⚖ 176 KB

## Abstract [__phenyl__‐^13^C~6~]Lachnanthocarpone ([__phenyl__‐^13^C~6~]2,6‐dihydroxy‐9‐phenylphenalen‐1‐one), a hypothetical intermediate in the biosynthesis of various natural phenylphenalenones, was prepared in four steps using [U‐^13^C]bromobenzene to introduce the label. Based on related meth

An efficient synthesis of 5-(phenyl-13C6
An efficient synthesis of 5-(phenyl-13C6)-5-phenylhydantoin
✍ Jacques H. Poupaert; Martial Winand; P. Dumont 📂 Article 📅 1981 🏛 John Wiley and Sons 🌐 French ⚖ 129 KB

## Abstract A procedure is described to convert benzene‐ ^13^C~6~ into 5‐(phenyl‐ ^13^C~6~)‐5‐phenylhydantoin in 80% overall yield.

Synthesis of benzoxazole-[phenyl-13C6] b
Synthesis of benzoxazole-[phenyl-13C6] by directed ortho-metalation chemistry
✍ Volker Derdau 📂 Article 📅 2004 🏛 John Wiley and Sons 🌐 French ⚖ 97 KB

## Abstract A new method for the preparation of benzoxazole‐[phenyl‐^13^C~6~] (**1**) starting from aniline‐[^13^C~6~] (**4**) has been developed involving directed __ortho__‐metalation (D__o__M) chemistry. The synthesis comprises four steps and an overall yield of 39% was obtained. Copyright © 200

Rapid synthesis of a 13C6-benzothiazoliu
Rapid synthesis of a 13C6-benzothiazolium salt from 13C6-aniline
✍ Chris V. Galliford; Kimberly Voronin; David Hesk; David Koharski; Paul McNamara 📂 Article 📅 2011 🏛 John Wiley and Sons 🌐 French ⚖ 174 KB

6 -labeled aniline was used as a starting material for the facile synthesis of 13 C 6 -benzothiazolium salt (1).