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Synthesis of New 1H-Pyridazine Derivatives peri-Anellated with Acenaphthene and Acenaphthylene.

โœ Scribed by V. V. Mezheritskii; L. G. Minyaeva; R. V. Tyurin

Book ID
101985534
Publisher
John Wiley and Sons
Year
2006
Weight
15 KB
Volume
37
Category
Article
ISSN
0931-7597

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Synthesis of new acenaphthylene function
Synthesis of new acenaphthylene functional derivatives. 1. 1-(Trimethylsilyl)- and 1,2- and 1,5-bis(trimethylsilyl)acenaphthylenes and related compounds
โœ Laguerre, Michel; Felix, Guy; Dunogues, Jacques; Calas, Raymond ๐Ÿ“‚ Article ๐Ÿ“… 1979 ๐Ÿ› American Chemical Society ๐ŸŒ English โš– 531 KB

0.75 g, 15 mmol) and chlorotrimethylsilane (3.15 mL, 25 mmol) in dry acetonitrile (25 mL). The progress of the reactions was monitored by IR, and they were complete in 6-8 h. Pure silyl nitronates were obtained after workup and characterized by their NMR and IR spectra. Silyl nitronate of 6a: 1.0 g