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Synthesis of new acenaphthylene functional derivatives. 1. 1-(Trimethylsilyl)- and 1,2- and 1,5-bis(trimethylsilyl)acenaphthylenes and related compounds

โœ Scribed by Laguerre, Michel; Felix, Guy; Dunogues, Jacques; Calas, Raymond

Book ID
127310948
Publisher
American Chemical Society
Year
1979
Tongue
English
Weight
531 KB
Volume
44
Category
Article
ISSN
0022-3263

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Synthesis of new acenaphthylene function
Synthesis of new acenaphthylene functional derivatives. 1. 1-(Trimethylsilyl)- and 1,2- and 1,5-bis(trimethylsilyl)acenaphthylenes and related compounds
โœ Laguerre, Michel; Felix, Guy; Dunogues, Jacques; Calas, Raymond ๐Ÿ“‚ Article ๐Ÿ“… 1979 ๐Ÿ› American Chemical Society ๐ŸŒ English โš– 531 KB

0.75 g, 15 mmol) and chlorotrimethylsilane (3.15 mL, 25 mmol) in dry acetonitrile (25 mL). The progress of the reactions was monitored by IR, and they were complete in 6-8 h. Pure silyl nitronates were obtained after workup and characterized by their NMR and IR spectra. Silyl nitronate of 6a: 1.0 g