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Acid-catalyzed isomerization of 1,2-bis(trimethylsilyl)benzene and related compounds

✍ Scribed by Seyferth, Dietmar; White, David L.

Book ID
126150708
Publisher
American Chemical Society
Year
1972
Tongue
English
Weight
820 KB
Volume
94
Category
Article
ISSN
0002-7863

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Synthesis of new acenaphthylene functional derivatives. 1. 1-(Trimethylsilyl)- and 1,2- and 1,5-bis(trimethylsilyl)acenaphthylenes and related compounds
✍ Laguerre, Michel; Felix, Guy; Dunogues, Jacques; Calas, Raymond πŸ“‚ Article πŸ“… 1979 πŸ› American Chemical Society 🌐 English βš– 531 KB

0.75 g, 15 mmol) and chlorotrimethylsilane (3.15 mL, 25 mmol) in dry acetonitrile (25 mL). The progress of the reactions was monitored by IR, and they were complete in 6-8 h. Pure silyl nitronates were obtained after workup and characterized by their NMR and IR spectra. Silyl nitronate of 6a: 1.0 g