Synthesis of N-phenyl-4-hydroxyphenyl carbamate
✍ Scribed by Segal, Alexander; Lavers, G.; Van Duuren, Benjamin L.
- Book ID
- 125986171
- Publisher
- American Chemical Society
- Year
- 1970
- Tongue
- English
- Weight
- 114 KB
- Volume
- 15
- Category
- Article
- ISSN
- 0021-9568
No coin nor oath required. For personal study only.
📜 SIMILAR VOLUMES
The title compound, C~13~H~12~N~2~OS, was prepared by the reaction of (4-pyridyl)methanol with phenyl isothiocyanate and NaOH in a 1,4-dioxane solution. The asymmetric unit contains two independent molecules. The molecular structure and packing are stabilized by N—H...N intermolecular hydrogen-bond
The title compound, C 13 H 8 Cl 2 O 2 , crystallizes with two independent molecules in the asymmetric unit. Each of the two unique molecules is twisted about the C-C single bonds, making dihedral angles of 24.29 (5) and 73.01 (5) between the two rings. In the crystal structure, the molecules are int