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Synthesis of mevalonolactone from 4-(β-hydroxyethyl)-4-methyl-1,3-dioxane

✍ Scribed by M. S. Sargsyan; A. T. Manukyan; S. A. Mkrtumyan; A. A. Gevorkyan

Book ID: 104832834
Publisher: Springer
Year: 1990
Tongue: English
Weight: 160 KB
Volume: 26
Category: Article
ISSN: 0009-3130
DOI: 10.1007/bf00605192

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## Abstract 1‐(4‐Chlorobenzyl)‐3‐methyl‐3‐(2‐hydroxyethyl)‐thiourea labelled with ^14^C at its urea group was synthesised starting from potassium cyanide‐^14^C, via potassium thiocyanate‐^14^C, 4‐chlorobenzyl‐thiocyanate‐^14^C and 4‐chlorobenzyl‐isothiocyanate‐^14^C. The conditions of the isomerisa