Structure of 5-benzoylamino-5-methyl-4-oxo-1,3-dioxane
✍ Scribed by M. L. Główka; G. Gilli; V. Bertolasi
- Publisher
- Springer
- Year
- 1986
- Tongue
- English
- Weight
- 220 KB
- Volume
- 16
- Category
- Article
- ISSN
- 1572-8854
No coin nor oath required. For personal study only.
📜 SIMILAR VOLUMES
## Abstract For Abstract see ChemInform Abstract in Full Text.
Irrespective of the fact that 1,3-dioxans have been recently intensively stud. ied very little attention has been paid to the preparation of 4-0x0-1,3dioxans? s2Hennes and Gundiger2 synthesised some chlorinated derivatives in concentrated sulphuric acid starting from chloral hydrate and a chlorinate
## Abstract Methyl 2‐benzoylamino‐3‐oxobutanoate (3) was prepared from hippuric acid (1) which was converted with __N,N‐__dimethylacetamide and phosphorus oxychloride into 4‐(1‐dimethylaminoethylidene)‐2‐phenyl‐5(4__H__)‐oxazolone (2) followed by hydrolysis with hydrochloric acid in methanol. Compo
In the title compound, C 12 H 13 NO 4 , the phenyl and oxazolidine rings make a dihedral angle of 65.0 (1) . Weak C-HÁ Á ÁO hydrogen-bonding interactions lead to the formation of a chain parallel to the a axis.