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Synthesis of methyl 2- and 4-pyridyl disulfide from 2- and 4-thiopyridone and methyl methanethiosulfonate

โœ Scribed by Trevor M. Kitson; Kerry M. Loomes


Book ID
102626857
Publisher
Elsevier Science
Year
1985
Tongue
English
Weight
123 KB
Volume
146
Category
Article
ISSN
0003-2697

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Synthesis of 2-methyl-4(5)-nitro[15N1(3)
โœ Jerzy Suwiล„ski; Wojciech Szczepankiewicz ๐Ÿ“‚ Article ๐Ÿ“… 1996 ๐Ÿ› John Wiley and Sons ๐ŸŒ French โš– 330 KB ๐Ÿ‘ 1 views

A simple four-stage conversion of 2-1nethyl-4(5>nitroimidazole to 2-methyl-4(5)-nitr0['~N""]imidazole is reported. The method consists in N-nitration of the initial compound to ?-methyl-1,4-dinitroimidazole, treating the latter with ["Nlglycine and N-dealkylation of the obtained (~-rnethyl-4-nitro[~