Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.005 A Ê Disorder in main residue R factor = 0.064 wR factor = 0.136 Data-to-parameter ratio = 12.4 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Synthesis and Crystal Structure of 3-Methyl-4-phenyl-5-(2-pyridyl)-1,2,4-triazole
✍ Scribed by Chunyi Liu; Zuoxiang Wang; Hailian Xiao; Yan Lan; Xiaomin Li; Songpei Wang; Jie Tang; Zhengping Chen
- Publisher
- Springer
- Year
- 2009
- Tongue
- English
- Weight
- 396 KB
- Volume
- 39
- Category
- Article
- ISSN
- 1572-8854
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📜 SIMILAR VOLUMES
In the crystal structure of the title compound, C 15 H 14 N 4 , all three aromatic rings, viz. 1,2,4-triazole, pyridine and benzene. The crystal structure shows that all three rings are not coplanar.
The title compound, C 21 H 19 N 5 , has been synthesized and characterized by single-crystal X-ray diffraction. The dihedral angle between the benzene and triazole rings is 123.0 (5) . The triazole ring forms dihedral angles of 36.5 (5) and 50.1 (5) with the two pyridyl rings.
The title compound, C 14 H 12 N 4 , is a disubstituted 1,2,4-triazole derivative. The triazole ring is planar and its dihedral angles with the attached pyridyl and methylphenyl rings are 25.2 (3) and 66.9 (3) , respectively. The crystal structure is stabilized by a number of CÐHÁ Á ÁN hydrogen bonds
The title compound, C 19 H 13 ClN 4 , was synthesized by the condensation of isonicotinohydrazide and N-(4-clorophenyl)benzimidoyl chloride in N,N-dimethylacetamide. In the title molecule, the triazole ring is oriented at dihedral angles of 34.64 (2), 30.97 (3) and 71.82 (3) with respect to the pyri