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Synthesis of macroheterocyclic analogs of dibenzocrown-compounds. 3. 18-Membered oxathiazacrown-compounds

✍ Scribed by A. A. Formanovskii; I. V. Mikhura; S. A. Sokolovskii; P. B. Terent'ev

Book ID
104781156
Publisher
Springer US
Year
1989
Tongue
English
Weight
416 KB
Volume
25
Category
Article
ISSN
0009-3122

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2-(l-Adamantyl)-2-hydroximinoacetonitrile Oxide (IV). A solution of K3Fe(CN) 6 (7.4 g, 22.5 mmole) and KOH (1.26 g, 22.5 mmole) in water (67 ml) was added dropwise with stirring to a solution of glyoxime la (2 g, 9 mmole) in ether (60 ml). The reactionmixture was stirred for 2 h at 25~ the ether lay