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Synthesis of Flexible Bis-Intercalating Ruthenium(II) Complexes

✍ Scribed by Craig R. Brodie; Janice R. Aldrich-Wright

Publisher
John Wiley and Sons
Year
2007
Tongue
English
Weight
279 KB
Volume
2007
Category
Article
ISSN
1434-1948

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πŸ“œ SIMILAR VOLUMES

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## Abstract Symmetrical, mononuclear bis(acetylido)ruthenium(II) complexes were prepared by the reaction of [__trans__‐RuMe~2~(dmpe)~2~] [dmpe = 1,2‐bis(dimethylphosphanyl)ethane] with terminal alkynes. The complexes were characterised by multinuclear NMR spectroscopy and X‐ray crystallography. In

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## Abstract Terminal acetylenes react with __cis__‐RuMe~2~(PMe~3~)~4~ to form the bis(acetylido) complexes __cis__/__trans__‐Ru(C≑CR)~2~(PMe~3~)~4~ in good yield. The structures of __trans__‐2 (R = Ph), __cis__‐3 (R = __p__‐C~6~H~4~‐OMe), __trans__‐4 (R = __p__‐C~6~H~4~‐Me), __cis__‐6 (R = Me), __t