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Synthesis of Enantiopure Aliphatic Acetylene Alcohols and Determination of Their Absolute Configurations by 1H NMR Anisotropy and/or X-ray Crystallography

✍ Scribed by Satoshi Sekiguchi; Megumi Akagi; Junpei Naito; Yoko Yamamoto; Hiromi Taji; Shunsuke Kuwahara; Masataka Watanabe; Yoshiki Ozawa; Koshiro Toriumi; Nobuyuki Harada

Publisher: John Wiley and Sons
Year: 2008
Tongue: English
Weight: 513 KB
Volume: 2008
Category: Article
ISSN: 1434-193X
DOI: 10.1002/ejoc.200800012

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## Abstract __meta__‐Substituted diphenylmethanols were enantioresolved by the method of chiral phthalic acid yielding enantiopure alcohols. Their absolute configurations were unambiguously determined by X‐ray crystallography of chiral phthalate esters and/or by the ^1^H NMR anisotropy method using