๐”– Bobbio Scriptorium
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Synthesis of deterium labeled plant ethylene precursor

โœ Scribed by Kye Chun Nam; Henry Rapoport

Book ID
102371198
Publisher
John Wiley and Sons
Year
1995
Tongue
French
Weight
304 KB
Volume
36
Category
Article
ISSN
0022-2135

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โœฆ Synopsis

Synthetic methods for the preparation of @ -deuterium labeled 2-keto-4-methylbutyric acid were investigated. Vinyl chloride was first reacted with the ethyl oxalyl chloride moiety using aluminum chloride as condensing agent and the addition of methyl mercaptan followed. Deuterium labeling was achieved by using NaBD4 reduction in pyridine.

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