𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Synthesis of carbon-14 labelled S-ethyl hexahydro-1H-azepine-1-carbothiolate

✍ Scribed by A. D. Gutman; D. R. Baker; M. E. Brokke

Publisher
John Wiley and Sons
Year
1966
Tongue
French
Weight
196 KB
Volume
2
Category
Article
ISSN
0022-2135

No coin nor oath required. For personal study only.

✦ Synopsis

labelled in the ethyl moiety and in the azepine ring with carbon-14 was prepared to facilitate residue and metabolism studies. The ethyl labeled compound was prepared in 86% yield and 99+% radiochemical purity. The azepine labeled material was prepared in 60% yield and 99+% radiochemical purity.

📜 SIMILAR VOLUMES

Synthesis of carbon-14 labeled 1,4-benzo
Synthesis of carbon-14 labeled 1,4-benzodiazepines. IV. Carbon-13 and carbon-14 labeled 8-chloro-1-(2-dimethylamino)ethyl-6-phenyl-4H-s-triazolo[4,3-a][1,4]-benzodiazepine tosylate
✍ Richard S. P. Hsi; Wayne T. Stolle 📂 Article 📅 1981 🏛 John Wiley and Sons 🌐 French ⚖ 341 KB

## Abstract Carbon‐13 and carbon‐14 labeled forms of the title compound have been prepared from the correspondingly labeled forms of 8‐chloro‐1‐methyl‐6‐phenyl‐4H‐__s__‐triazolo[4,3‐a][1,4]benzodiazepine (__3__)Alprazolam is the generic USAN name for this compound. . A modified and more convenient

Synthesis of carbon-14 labeled 1, 4-benz
Synthesis of carbon-14 labeled 1, 4-benzodiazepines
✍ Richard S. P. Hsi 📂 Article 📅 1973 🏛 John Wiley and Sons 🌐 French ⚖ 248 KB 👁 1 views

## Abstract Reaction of 7‐chloro‐1, 3‐dihydro‐5‐phenyl‐2H‐1, 4‐benzodiazepine ‐2‐thione (Ia) and 7‐chloro‐5‐(2‐chlorophenyl)‐1, 3‐dihydro‐2H, 1, 4‐benzodiazepine‐2‐thione (Ib) with hydrazine produces. respectively, 7‐chloro‐5‐phenyl‐3H‐1, 4‐benzo‐diazepin‐2‐yl hydrazin (IIa) and 7‐chloro‐5(2‐chlorp

Synthesis of carbon - 14 labeled 1-β -D-
Synthesis of carbon - 14 labeled 1-β -D-arabinofuranosylcytosine
✍ Richard S. P. Hsi 📂 Article 📅 1972 🏛 John Wiley and Sons 🌐 French ⚖ 215 KB

The s y t h e s i s of carbon-14 labeled l-ir-3-ar~,'lI-7f~r~c.q, Icdtosine and i t s hydrochloride salt i s described. i n four steps from bariwn carbonats-'4C, are labeterl in ;ve Z-7 position of the pyrimidine ring.

Synthesis of14C-labeled hexahydro-1,3,5-
Synthesis of14C-labeled hexahydro-1,3,5-trinitro-1,3,5-triazine(RDX)
✍ Károly Horváth; William L. Alworth 📂 Article 📅 1993 🏛 John Wiley and Sons 🌐 French ⚖ 184 KB 👁 1 views

## Abstract ^14^C‐labeled hexahydro‐1,3,5‐trinitro‐1,3,5‐triazine (2, RDX) was prepared by nitrolysis of hexahydro‐1,3,5‐tripropionyl‐1,3,5‐triazine (1) for bioenvironmental studies. 1 was synthesized from paraformaldehyde and propionitrile by a modified method reported earlier.