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SYNTHESIS OF BIOLOGICAL MARKERS IN FOSSIL FUELS 5. A SYNTHESIS OF 5α-CHOLAN-24-OIC ACID

✍ Scribed by Demir, Ayhan; Sabol, Mark; Jeganathan, Alwarsamy; Dolence, Eric Kurt; Watt, David; Moldowan, J. Michael

Book ID
127026627
Publisher
Taylor and Francis Group
Year
1987
Tongue
English
Weight
526 KB
Volume
19
Category
Article
ISSN
0030-4948

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## Abstract A short, practical, multigram‐scale synthesis of C3α‐NHAlloc, C12α‐NHBoc‐diamino‐5β‐cholan‐24‐oic acid **2** was developed, applying a new, straightforward synthetic strategy. Key features are the conservation of the carboxyl moiety at C24 during oxime reduction, the late differentiatio