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Synthesis of 3α,7α,14α-Trihydroxy-5β-cholan-24-oic Acid: A Potential Primary Bile Acid in Vertebrates.

✍ Scribed by Genta Kakiyama; Takashi Iida; Takaaki Goto; Nariyasu Mano; Junichi Goto; Toshio Nambara

Publisher
John Wiley and Sons
Year
2004
Weight
134 KB
Volume
35
Category
Article
ISSN
0931-7597

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Short Synthesis of Orthogonally Protected 3α,12α-Diamino-5β-cholan-24-oic Acid, a Dipodal Steroid Scaffold for Combinatorial Chemistry
✍ Dieter Verzele; Annemieke Madder 📂 Article 📅 2007 🏛 John Wiley and Sons 🌐 English ⚖ 128 KB

## Abstract A short, practical, multigram‐scale synthesis of C3α‐NHAlloc, C12α‐NHBoc‐diamino‐5β‐cholan‐24‐oic acid **2** was developed, applying a new, straightforward synthetic strategy. Key features are the conservation of the carboxyl moiety at C24 during oxime reduction, the late differentiatio