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Synthesis of Azocino[5,4- b ]indoles via Gold-Catalyzed Intramolecular Alkyne Hydroarylation

✍ Scribed by Peshkov, Vsevolod A.; Pereshivko, Olga P.; Eycken, Erik V. Van der

Book ID
120341134
Publisher
John Wiley and Sons
Year
2012
Tongue
English
Weight
271 KB
Volume
354
Category
Article
ISSN
1615-4150

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Synthesis of the Azocino[cd]indole Frame
Synthesis of the Azocino[cd]indole Framework through Pd-Catalyzed Intramolecular Acetylene Hydroarylation
✍ Vsevolod A. Peshkov; Sofie Van Hove; Pavel A. Donets; Olga P. Pereshivko; Kristo πŸ“‚ Article πŸ“… 2011 πŸ› John Wiley and Sons 🌐 English βš– 372 KB

## Abstract The regio‐ and stereoselective construction of the azocino[__cd__]indole core was achieved by applying a Pd‐catalyzed intramolecular acetylene hydroarylation protocol. The applicability of a similar strategy for the synthesis of the azepino[__b__]indole framework is demonstrated.

Synthesis of pyrimido[4,5-b]indoles and
Synthesis of pyrimido[4,5-b]indoles and benzo[4,5]furo[2,3-d]pyrimidines via palladium-catalyzed intramolecular arylation
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Various pyrimido[4,5-b] indoles and benzo [4,5]furo [2,3-d]pyrimidines were synthesized via a palladium-catalyzed intramolecular arylation of pyrimidine substrates. Thus, 4-aryloxy-or 4-anilino-5-iodopyrimidines were treated with Pd(OAc) 2 (PPh 3 ) 2 and base in DMF to give the regioselective cycli