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Synthesis of a protected derivative of (2R,3R)-β-hydroxyaspartic acid suitable for Fmoc-based solid phase synthesis

✍ Scribed by France, Boyaud; Bruno, Viguier; Nicolas, Inguimbert

Book ID
118049462
Publisher
Elsevier Science
Year
2013
Tongue
French
Weight
350 KB
Volume
54
Category
Article
ISSN
0040-4039

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Fmoc-(R)-b -HomoAsp(OtBu)-OH was used for the synthesis of both (R) and (S) enantiomers of various Fmoc-protected 3-substituted 1,2,4-oxadiazole-containing b 3 -amino acids. The 1,2,4-oxadiazole heterocycle was formed using sodium acetate, a Fmoc-compatible and efficient catalyst for cyclodehydrati