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Synthesis of a 3-deoxy-d-manno-octulosonic acid (KDO) building block from d-glucose via fermentation

✍ Scribed by Camci-Unal, Gulden; Mizanur, Rahman M.; Chai, Yonghai; Pohl, Nicola L. B.

Book ID: 118165269
Publisher: Royal Society of Chemistry
Year: 2012
Tongue: English
Weight: 642 KB
Volume: 10
Category: Article
ISSN: 1477-0520
DOI: 10.1039/c2ob25168j

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A Silicon-Mediated Synthesis of 3-Deoxy-D-manno-octulosonic Acid (KDO). -Starting from commercially available D-mannitol (I), the synthesis of KDO ammonium salt (VII) includes, as key steps, a silicon-mediated epoxide ring opening reaction of (II) and silicon-induced lactonization of carbonate (V) w