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Synthesis of 6- and 9-Ethylocatadecanoic Acids

✍ Scribed by Dario Dragas; Hanafi Tanojo; Johannes Brussee; Hans E. Junginger; Harry E. Boddé

Publisher
John Wiley and Sons
Year
1996
Tongue
English
Weight
347 KB
Volume
329
Category
Article
ISSN
0365-6233

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📜 SIMILAR VOLUMES

ChemInform Abstract: Synthesis of 6- and
ChemInform Abstract: Synthesis of 6- and 9-Ethyloctadecanoic Acids.
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## Abstract Starting from divarinol (**4**) using previously published procedures, (±)‐6,6‐[^2^H~6~]Dimethyl‐11‐nor‐Δ^9^THCV‐9‐carboxylic acid (**3**) was synthesized for use as an internal standard in GC/MS analysis of 11‐nor‐Δ^9^THCV‐9‐carboxylic acid (**2**). The detection of **2** distinguishes

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## Abstract 9(10)‐Bromo‐cis‐9‐octadecenoic acid, m. p. 36.7° C, was prepared by dehydrobromination of threo‐9,10‐dibromo‐stearic acid with bases and by polar addition of hydrogen bromide to stearolic acid. The trans isomer, m. p. 6°–8° C, was obtained from the corresponding erythro‐dibromide. Both