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Synthesis of 5-amino[carboxyl-14C]salicylic acid

✍ Scribed by Ole Jørgensen; Susanne Petersen; Lars Carlsen

Publisher
John Wiley and Sons
Year
1987
Tongue
French
Weight
121 KB
Volume
24
Category
Article
ISSN
0022-2135

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✦ Synopsis

Improvements have baen made to the synthesis of 5-aminasalicylic wid (S-ASA) in order to make it applicable for the small-scale synthesis of 5-smidcerboxvl-l ~l s a l i c y l i c acid.

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Synthesis of 2,3-dihydroxybenzoic acid -
Synthesis of 2,3-dihydroxybenzoic acid - (carboxyl-14C)
✍ M. G. Sundaram 📂 Article 📅 1981 🏛 John Wiley and Sons 🌐 French ⚖ 194 KB

## Abstract 2,3‐Dihydroxybenzoic acid‐(carboxyl‐^14^C) can be synthesized in high overall yield from commercially‐available 2,3‐dimethoxybenzoic acid. The synthetic route features the application of a Curtius rearrangement, the thermal decomposition of a carboxylic acid azide to an isocyanate. The