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Synthesis of 4,5-dihydro-1,4-benzothiazepine derivatives via ring expansion

✍ Scribed by L. Fodor; J. Szabó; G. Bernáth; L. Párkányi; P. Sohár

Publisher
Elsevier Science
Year
1981
Tongue
French
Weight
132 KB
Volume
22
Category
Article
ISSN
0040-4039

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Solid phase synthesis of 1,4-benzothiaze
Solid phase synthesis of 1,4-benzothiazepin-5-one derivatives
✍ Adel Nefzi; Nhi A Ong; Marc A Giulianotti; John M Ostresh; Richard A Houghten 📂 Article 📅 1999 🏛 Elsevier Science 🌐 French ⚖ 199 KB

The solid phase synthesis of 1,4-benzothiazepin-5-one derivatives, resulting from the reaction of resin-bound protected cysteine with 2-fluoro-5-nitro-benzoic acid followed by a reductive aikylation and an intra molecular cyclization, is described.