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Synthesis of 4-Hydroxyquinolines. III. A Direct Synthesis of β-Substituted Acrylic Esters1

✍ Scribed by Snyder, H. R.; Jones, Robert E.

Book ID
115513271
Publisher
American Chemical Society
Year
1946
Tongue
English
Weight
345 KB
Volume
68
Category
Article
ISSN
0002-7863

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Nucleophilic substitution of vinylic iodide of methyl 2-(1-hydroxyalkyl)-3-iodo prop-2-enoates 8 in the presence of magnesium dialkyl cuprates generated in situ provided a stereoselective methodology for the synthesis of infrequent b-substituted Baylis-Hillman products.