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Synthesis of 4-hydroxy-1-thiocoumarin derivatives-1: An efficient synthesis of thioflocoumafen

โœ Scribed by Jae Chul Jung; Ju Cheun Kim; Oee Sook Park; Bong Suek Jang


Book ID
105672444
Publisher
Springer
Year
1999
Tongue
English
Weight
360 KB
Volume
22
Category
Article
ISSN
0253-6269

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A simple and environmental friendly microwave irradiation method is devised for the synthesis of derivatives of 1,3,4-oxadiazoles viz., 6a-e and 7h-q in 75-90% yield. Structures of the newly synthesised compounds were confirmed by physical, analytical and spectral (ir, 1 H and 13 C nmr and ms) data