Synthesis of 4-Acetamido-1,2,3,5-tetra-O-acetyl-4-deoxy-D-ribofuranose. A Pyrrolidine Sugar 1-3
โ Scribed by Reist, Elmer J.; Gueffroy, Donald E.; Goodman, Leon
- Book ID
- 126864720
- Publisher
- American Chemical Society
- Year
- 1965
- Tongue
- English
- Weight
- 249 KB
- Volume
- 87
- Category
- Article
- ISSN
- 0002-7863
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๐ SIMILAR VOLUMES
We have previously reported' the synthesis of 1,2,3-tri-O-acetyGI,Sdideoxy-4-C-[(R,S)-phenylphosphinyl] -o&3-D-ribo-and -L-lyxo-furanoses (4) by the sequence of 1 -+ 2 + 3 + 4. However, this method could not be applied to a synthesis of 4deoxy-\*To whom correspondence may be addressed.
## Crystals of the tetrasaccharide, (2,3,4,6-tetra-0acetyl-fi-D-ghxopyranosyl~-(1 + 3)-[2,3,4,6-tetra-O-acetyI+LD-gIucopyranosyI-(1 --t 6)]-(2,4-di-0-acetyl-g\_D-glucopyranosyl)-1 --) 3)-1,2,4,6-tetrad-acetyl$?-n-ghicopyranose, belong to tge monoclinic system, space group P2,, with a = 12.709(4),