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The high resolution mass spectrum of 2-acetamido-1,3,4,6-tetra-O-acetyl-2-deoxy-α-D-glucopyranose

✍ Scribed by Ralph C. Dougherty; Derek Horton; Kerstin D. Philips; Joseph D. Wander

Publisher
John Wiley and Sons
Year
1973
Tongue
English
Weight
656 KB
Volume
7
Category
Article
ISSN
1076-5174

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## Abstract Methyl‐2‐acetamido‐4,6‐di‐__O__‐acetyl‐3‐__S__‐acetyl‐2‐deoxy‐3‐thio‐α‐D‐mannopy‐ranoside has been synthesized by conversion of methyl 2‐amino‐2‐deoxy‐4,6‐__O__‐benzylidene‐α‐D‐altropyranoside into the corresponding 3‐__O__‐methanesulfony1‐2‐__N__‐[(methylthio)thiocarbonyl]derivative fo

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The crystal structure of a-D-Manp-(1 +3)-/?-D-Manp-( 1-+4)-a-D-GlcNAcp has been determined by the direct method using the multi-solution, tangentzformula, and "magic integer" procedures. The space group is P2,, and 2 molecules are in the unit cell with c1 = 9.894 ( 5), b = 10.372 (6), c = 11.816 (6)