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Synthesis of [3H]cyfluthrin

✍ Scribed by Ulrich Pleiß; Johannes Römer; Rudolf Thomas

Publisher: John Wiley and Sons
Year: 1993
Tongue: French
Weight: 295 KB
Volume: 33
Category: Article
ISSN: 0022-2135
DOI: 10.1002/jlcr.2580331009

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✦ Synopsis

Abstract

For the elucidation of the distribution and biotransformation of Cyfluthrin in tse‐tse flies the tritium‐labelled compound was needed. A brominated precursor was dehalogenated with tritium gas using a special noble metal catalyst to give the desired [^3^H]Cyfluthrin. The labelling position was confirmed by ^3^H‐NMR spectroscopy. After synthesis and purification, the [^3^H]Cyfluthrin obtained showed a specific activity of 23.7 Ci/ mmol (877 GBq/mmol).

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