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Synthesis of 2,6-dimethyl-l,2,3,4-tetrahydronaphthalene-4-13C and 2,6-dimethylnaphthalene-413C

✍ Scribed by D. L. Bymaster; R. E. Pickering; T. K. Dobbs; E. J. Eisenbraun

Publisher
John Wiley and Sons
Year
1986
Tongue
French
Weight
334 KB
Volume
23
Category
Article
ISSN
0022-2135

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✦ Synopsis

The synthesis of specifically labeled 6,4-dimethyl-benzenebutanoic acid-l-C, 3,4-Dihydro-3,7-dirnethyl-l(2fJ)-naph-thalen~ne-L-~~C, 2,6-dimethyl-l,2,3,4-tetrahydronaphthalene-4-13 C and Z,L-dimethylnaphthale~~e-i-'~c from Diethyl 2-(4methylphenyl)-2-methylpropanediate is described.

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## Abstract The first synthesis of doubly labeled, [2‐^13^C, 4‐^13^C]‐(2__R__,3__S__)‐catechin 15 and [2‐^13^C, 4‐^13^C]‐(__2R__,3__R__)‐epicatechin 18 starting from labeled 2‐hydroxy‐4, 6‐bis(benzyloxy)acetophenone 3 and labeled 3, 4‐bis(benzyloxy)‐benzaldehyde 7 are described. Copyright Β© 2010 Jo