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Synthesis of 2,4,6(1H,3H,5H)-pyrimidinetrione-5-carboxaldehyde

✍ Scribed by A. V. Erkin; V. I. Krutikov

Book ID
111460491
Publisher
Springer
Year
2010
Tongue
English
Weight
119 KB
Volume
80
Category
Article
ISSN
1070-3632

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## Abstract (__R__)‐5‐(diallylamino)‐5,6‐dihydro‐4__H__‐imidazo[4,5,1‐__ij__]quinolin‐2(1__H__)‐one (__12b__) was prepared in 9% overall yield from 3‐aminoquinoline. Reaction of __12b__ in ethyl acetate with tritium gas in presence of a 5% platinum on carbon catalyst afforded a mixture of (__R__)‐5