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Electrocatalytic trimerization of N,N′-dialkylbarbituric acids: facile and efficient way to 2′H-5,5′:5′,5″-terpyrimidine-2,2′,2″,4,4′,4″,6,6′,6″-(1H,1′H,1″H,3H,3′H,3″H,5H,5″H)-nonone framework

✍ Scribed by Vereshchagin, Anatoly N.; Elinson, Michail N.; Dorofeeva, Evgeniya O.; Bushmarinov, Ivan S.; Gorbunov, Sergey V.; Belyakov, Pavel A.; Chizhov, Alexander O.; Nikishin, Gennady I.


Book ID
119328547
Publisher
Elsevier Science
Year
2012
Tongue
English
Weight
571 KB
Volume
363-364
Category
Article
ISSN
1381-1169

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Synthesis of (R)-5-(Di[2,3-3H2]propylami
✍ Malcolm W. Moon; Richard S. P. Hsi 📂 Article 📅 1992 🏛 John Wiley and Sons 🌐 French ⚖ 542 KB

## Abstract (__R__)‐5‐(diallylamino)‐5,6‐dihydro‐4__H__‐imidazo[4,5,1‐__ij__]quinolin‐2(1__H__)‐one (__12b__) was prepared in 9% overall yield from 3‐aminoquinoline. Reaction of __12b__ in ethyl acetate with tritium gas in presence of a 5% platinum on carbon catalyst afforded a mixture of (__R__)‐5