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Synthesis of 14C-labeled eschenmoser's salt: Dimethyl([14C]methylene)ammonium iodide

✍ Scribed by Lidia Kupczyk-Subotkowska; Henry J. Shine

Publisher
John Wiley and Sons
Year
1993
Tongue
French
Weight
169 KB
Volume
33
Category
Article
ISSN
0022-2135

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✦ Synopsis

Abstract

A six step synthesis of dimethyl([^14^C]methylene)ammonium iodide (Eschenmoser's salt) is described. Sodium [2‐^14^C]acetate was used as the starting material. The overall yield of the final product was 30% with specific activity 8 mCi/mol.

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