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Synthesis of 1,4-dihydro-4-methyl-1-phenyl-5H-1,3,4-benzotriazepin-5-ones

✍ Scribed by Norton P. Peet; Shyam Sunder


Book ID
112123853
Publisher
Journal of Heterocyclic Chemistry
Year
1976
Tongue
English
Weight
384 KB
Volume
13
Category
Article
ISSN
0022-152X

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Facile synthesis of model 1,4-dihydro-1H
✍ Bassam A. Abu Thaher; Jalal A. Zahra; Mustafa M. El-Abadelah πŸ“‚ Article πŸ“… 2002 πŸ› Journal of Heterocyclic Chemistry 🌐 English βš– 48 KB

## Abstract 2‐Aminobenzoic acid reacts readily, in the presence of triethylamine, with hydrazonoyl chlorides (**5a‐c**) (precursors of the reactive nitrile imine 1,3‐dipolar species) to afford high yields of the corresponding acyclic amidrazone adducts (**6a‐c**). The latter adducts undergo, in THF