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Synthesis of 4,5-dihydro-4-phenyl-3H-1,3,4-benzotriazepines

✍ Scribed by Lawrence L. Martin; Marc N. Agnew; Linda L. Setescak

Book ID: 112127945
Publisher: Journal of Heterocyclic Chemistry
Year: 1985
Tongue: English
Weight: 235 KB
Volume: 22
Category: Article
ISSN: 0022-152X
DOI: 10.1002/jhet.5570220436

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## Abstract 2‐Aminobenzoic acid reacts readily, in the presence of triethylamine, with hydrazonoyl chlorides (**5a‐c**) (precursors of the reactive nitrile imine 1,3‐dipolar species) to afford high yields of the corresponding acyclic amidrazone adducts (**6a‐c**). The latter adducts undergo, in THF