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5-Aryl-1,3-dihydro-2H-1,3,4-benzotriazepin-2-ones

✍ Scribed by Sulkowski, Theodore S.; Childress, Scott J.

Book ID: 120886726
Publisher: American Chemical Society
Year: 1964
Tongue: English
Weight: 154 KB
Volume: 7
Category: Article
ISSN: 0022-2623
DOI: 10.1021/jm00333a046

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## Abstract 2‐Aminobenzoic acid reacts readily, in the presence of triethylamine, with hydrazonoyl chlorides (**5a‐c**) (precursors of the reactive nitrile imine 1,3‐dipolar species) to afford high yields of the corresponding acyclic amidrazone adducts (**6a‐c**). The latter adducts undergo, in THF