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Synthesis of 13C4-labelled oxidized metabolites of the carcinogenic polycyclic aromatic hydrocarbon benzo[a]pyrene

✍ Scribed by Anhui Wu; Daiwang Xu; Ding Lu; Trevor M. Penning; Ian A. Blair; Ronald G. Harvey

Book ID
116909553
Publisher
Elsevier Science
Year
2012
Tongue
French
Weight
806 KB
Volume
68
Category
Article
ISSN
0040-4020

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✍ J. Ernest Simpson; Guido H. Daub; David L. Vanderjagt πŸ“‚ Article πŸ“… 1980 πŸ› John Wiley and Sons 🌐 French βš– 240 KB

## Abstract The synthesis of benzo[a]pyrene‐6‐^13^C is described. Perinaphthane was converted to 6‐benzoyl‐carbonyl‐^13^C‐perinaphthane which was cyclized to 2,3‐dihydrobenzo[a]pyren‐6(1H)‐one‐6‐^13^C. Subsequent reduction of the ketone followed by dehydration and dehydrogenation gave benzo[a]pyren