## Abstract Procedures are described for the synthesis of 1,3,5‐trinitro‐1,3,5‐triazacyclohexane (RDX), 1,3,5,7‐tetranitro‐1,3,5,7‐tetraazacyclooctane (HMX) fully labeled with nitrogen‐15.
Synthesis of 1,3,5-TRI(nitro-15N)-1,3,5-hexahydrotriazine, RDX-(15NO2)3
✍ Scribed by Michael E. Sitzmann
- Publisher
- John Wiley and Sons
- Year
- 1985
- Tongue
- French
- Weight
- 144 KB
- Volume
- 22
- Category
- Article
- ISSN
- 0022-2135
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✦ Synopsis
The synthesis o f 1,3,S-t r i ( n i tro-1SN)-l,3,S-hexahydrotri a z i ne, RDX-( 15 N02)3, by n i t r o l y s i s o f 1,3,5-t r i acetyl -1,s ,5-hexahydrot r i a z i ne i s described. A method f o r recovery o f t h e nitrogen-15 l a b e l l e d n i t r i c a c i d n o t consumed i n t h e n i t r o l y s i s i s a l s o provided.
📜 SIMILAR VOLUMES
## Abstract A series of novel neonicotinoids analogs were designed by modifying the pharmacophore of imidacloprid to 1,3,5‐hexahydrotriazine conjugated to nitroimine (NNO~2~) and introducing the phenyl or arylmethyl at the 5‐position, and their insecticidal activities were evaluated. Introducing a
A simple four-stage conversion of 2-1nethyl-4(5>nitroimidazole to 2-methyl-4(5)-nitr0['~N""]imidazole is reported. The method consists in N-nitration of the initial compound to ?-methyl-1,4-dinitroimidazole, treating the latter with ["Nlglycine and N-dealkylation of the obtained (~-rnethyl-4-nitro[~