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Synthesis of 1,3-Cyclohexadienes by Tandem Diene—Alkyne Metathesis: Improved Procedure.

✍ Scribed by Mark D. Middleton; Steven T. Diver

Book ID
101972910
Publisher
John Wiley and Sons
Year
2005
Weight
26 KB
Volume
36
Category
Article
ISSN
0931-7597

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✍ Atsushi Kinoshita; Norikazu Sakakibara; Miwako Mori 📂 Article 📅 1999 🏛 Elsevier Science 🌐 French ⚖ 795 KB

A novel 1,3-diene synthetic method from alkyne and ethylene was developed using ruthenium-catalyzed enyne metathesis. The reaction procedure is very simple: A CH2CI 2 solution of alkyne was stirred at room temperature under ethylene gas (1 atm.) in the presence of a catalytic amount of ruthenium ben