Synthesis of 1,1,3,3-Tetraalkylisoindolines Using a Microwave-Assisted Grignard Reaction
β Scribed by Foitzik, Richard C.; Bottle, Steven E.; White, Jonathan M.; Scammells, Peter J.
- Book ID
- 120349261
- Publisher
- Commonwealth Scientific and Industrial Research Organisation Publishing
- Year
- 2008
- Tongue
- English
- Weight
- 236 KB
- Volume
- 61
- Category
- Article
- ISSN
- 0004-9425
- DOI
- 10.1071/CH08008
No coin nor oath required. For personal study only.
π SIMILAR VOLUMES
## Abstract The application of microwave technique has been extended successfully for the first time to the synthesis of a representative class of azaphospholes, viz. 1,3βbis(alkoxycarbonyl)β1,3βazaphospholo[5,1β__a__]isoquinolines (**__2__**), which occurs rapidly giving higher yields. Stereoselec
Ring-closure of 1,3-azadienes to 13-1actam rings is efficiently and quickly carried out under solvent-free conditions in an open-vessel microwave system. The synthesis of N-tert-butyldimethylsilyl azetidinones is reported.